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why add sodium sulphate incompound for rotary evaporator

what is the usage of a rotary evaporator (rotovap)? - Lab

Rotary evaporation is a technique most commonly used in organic chemistry to remove a solvent from a higher-boiling point compound of interest. The rotary evaporator, or “ rotovap “, was invented in 1950 by the chemist Lyman C. Craig. The primary use of a rotovap is to dry and purify samples for downstream appliions.

OPCW Proficiency Test: A Practical Approach Also - Hindawi

The dichloromethane phase dry with sodium sulfate, and evaporate it on a rotary evaporator to dryness for preparation of methyl or TMS derivative, using etheral CH 2 N 2 /CH 3 OH or BSTFA/CH 3 CN, appropriately. (iv) General Procedures to Synthesize O,S-Dialkyl Alkylphosphonates.

Reduction of Carbonyl Compounds | Organic Chemistry II - JoVE

Once complete, add 10 mL of water to the reaction mixture. Transfer into a separatory funnel and extract with ethyl acetate (2x 30 mL). Dry with DI water (1x 30 mL) and with brine (1x 30 mL). Dry over sodium sulfate and filter into a round-bottom flask. Evaporate the solvent on a rotary evaporator. Take a TLC and IR of the reduction product. 3.

S THF, 80 C - Michigan Technological University

Dry the organic layer with sodium sulphate and concentrate under vacuum to obtain 3. To destroy the volatile thiols place NaOCl traps (Laundry Bleach~ 5% NaOCl or High-Test Hypochlorite (HTH) 30% NaOCl) in between the vacuum pump (self contained mechanical pump) and rotary evaporator as shown in Fig1. Collect the pump water for disposal treatment.

Chemical composition, in vitro cytotoxicity and anti-free

aqueous solution formed by ammonium sulphate (20%), and meta-phosphoric acid (2%) in same amounts and left for 15 minutes to de separated and constants. The upper phase ethyl acetate fraction was taken and dried by adding a sufficient amount of anhydrous sodium sulphate and then evaporated to dryness using a rotary evaporator. The

Drying Organic Solutions

Usually, you will perform a wash with saturated sodium chloride solution to remove the bulk of the water before treating with an inorganic salt. Add a small amount of the solid drying agent directly to the organic solution. Swirl the solution. Observe …

Coluia University in the City of New York

The dry ether solution is evaporated by a rotary evaporator You may need to add several drops, as some solvents have a small, but significant, solubility in water. Dry your organic layer with sodium sulfate and gravity filter into a pre-weighed round-bottom flask. Evaporate the solvent using a rotovap and determine the mass of solid you

Persistence of Imidacloprid, Indoxacarb and Lada

Jul 07, 2018· rotary vacuum evaporator at 400C. After evaporation of DCM, the residues were dissolved in 2ml ethyl acetate. For cleanup of the extracted samples of imidacloprid, the chromatography column (50×1.5cm) was prepared by adding silica gel over 2cm layer of anhydrous sodium sulphate (Dharmurajan and Dikshit, 2010).

[Solved] You have a solution of your desired compound in

it will increase the volatility of your desired compound, causing some of it to be lost on the rotary evaporator. The more drying agent that is used, the more the compound may be irrecoverably lost. Question 4. This the correct sequence. 1. Wash the organic layer with brine. 2. Dry the organic layer with sodium sulphate. 3.

Sodium Sulfate - an overview | ScienceDirect Topics

Add sodium sulfate into the Envi-Carb cartridge to ca. 2 cm. Connect the cartridge to the top of the aminopropyl Sep-Pak cartridge in series. Fix the cartridge into a support to which a pear-shaped flask is connected. Condition the cartridge with 4 mL acetonitrile-toluene (3 + 1) before adding the sample.

SEPARATION OF A THREE COMPONENT MIXTURE: …

Rotary Evaporator (Text p 198-201) Purpose: Separation of benzoic acid, ethyl-4-aminobenzoate and naphthalene. C O OH C O OCH 2C H 3 NH 2 Dry the organic layer by adding anhydrous sodium sulfate a little at a time until it does not clump. The liquid should be clear and at least a little of the drying agent

US Patent Appliion for ORGANIC - Justia Patents Search

Jan 13, 2015· Then 2-chloropyridine (4.82 mL, 42.45 mmol) was added and continued to reflux for 72 h. Benzene was removed using rotary evaporator. Crude product was extracted with dichloromethane and washed with water. The organic layer was dried over anhydrous sodium sulphate and solvent was evaporated on the rotary evaporator under reduced pressure.

Isolation of Plant Pigments by Column Chromatography

Add 2-3 spatula of anhydrous sodium sulfate to remove traces of water that may be present in the crude extract. Filter off sodium sulfate from the crude extract using a funnel. The yellow and green pigments collected from the column are then concentrated by removing the solvents using a rotary evaporator.

Controlled Release Fertilizers And Nanotechnology Traces

The main synthetic or mineral fertilizers which are the sources of nitrogen (N), potassium(K), phosphate (P) are urea, ammonium sulfate, ammonium phosphate, phosphate rock, potassium chloride, super phosphates, calcium ammonium nitrate, potassium sulfate. Fertilizers could be in compound form (NP, PK, NPK).The most important drawback of

EXPERIMENT 2 SODIUM BOROHYDRIDE REDUCTION OF - …

The clear layer is the product and anhydrous sodium sulphate was added to remove moisture. Later rotary evaporator is used to remove the dichloromethane. OBJECTIVE 1. To investigate the reduction reaction of a ketone to an alcohol using sodium borohydride as the reducing agent. 2. To determine the percentage yield of the product produced.

Synthesis of 3-phenyl propionic acid (hydrocinnamic acid

Remove ethanol as much as possible by distillation under reduced pressure (rotary evaporator) on a water bath. Cool the flask contents to 20 °C, add 200 ml of water to it and shake well. Separate the upper layer of crude ester, dry it with anhydrous sodium sulphate and distil under reduced pressure.

What is the purpose of using the rotary evaporator? - Lab

The setup of a rotary evaporator The first step is to pour the solvent mixture and the compound you want to work on in a round bottom flask. It is advisable to fill the flask less than a half if you want to get the desired results. The second step is to fill …

Controlled Release Fertilizers And Nanotechnology Traces

The main synthetic or mineral fertilizers which are the sources of nitrogen (N), potassium(K), phosphate (P) are urea, ammonium sulfate, ammonium phosphate, phosphate rock, potassium chloride, super phosphates, calcium ammonium nitrate, potassium sulfate. Fertilizers could be in compound form (NP, PK, NPK).The most important drawback of

How can I test Sodium? Is there a test kit for sodium

Mar 02, 2016· Testing Sodium by Flame Photometer. An alternative method to test Sodium is by a flame photometer – these are benchtop units and cannot be used for portable testing, but they do offer very high accuracy and can measure a range of sample types including clinical samples. They also have the added benefit of being able to test other ions by

Lab 3 Report - Acid-Base Extraction Results and Discussion

Acid-Base Extraction. Results and Discussion: 1. T o remove the benzoic acid from the solution, a base, NaHCO 3, was added. This. compound reacted with the benzoic acid to form its conjugate base. The NaHCO 3. accepted a hydrogen from benzoic acid. Whe n benzoic acid became its conjugate base, it.

US2645561A - Sodium sulfate recovery - Google Patents

sodium sulfate liquor sulfuric acid acid water Prior art date 1948-11-23 Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.) Expired - Lifetime Appliion nuer US61612A Inventor Malm Lawrence Louis

CN112034080A - Method for detecting amide substances in

The invention discloses a method for detecting amide substances in water, relates to the field of detection methods of amide substances in the field of environmental detection, and aims to solve the problem that a detection and analysis method is lacked when a specific industrial site is polluted by the amide substances. The method comprises the following steps: the method …

LIQUID/LIQUID SEPARATION: EXTRACTION OF ACIDS OR …

11. Rinse the separatory funnel with an additional 5-mL of ether, and add that rinse to Flask 2. 12. Add sodium sulfate to Flask 2 and swirl. The amount required depends on how much water is in the mixture. Typically one full scoopula of sodium sulfate should suffice, but frequently additional drying agent is required.

CFR - Code of Federal Regulations Title 21 - Food and Drug

Jan 06, 2022· Evaporate the 40-percent benzene in hexane eluate on the rotary vacuum evaporator at 45 deg.C until only the n-hexadecane residue of 0.5 milliliter remains. Treat the n- hexadecane residue twice with the following wash step: Add 6 milliliters of purified isooctane and remove the solvents by vacuum evaporation at 45 deg.C to constant volume, i.e

Silica gel for column chromatography (particle size of 63

suction into a vacuum rotary evaporator flask. Collect the residue on the filter paper, add 50 mL of acetone, homogenize for 3 minutes, treat as described above, coine the filtrate in the vacuum rotary evaporator flask, and remove acetone at below 40°C. Transfer to a 300 mL separating funnel containing 100 mL of saturated sodium chloride

Organics Practicals

Nov 24, 2018· Shake the total product with 90 ml of water in a 250-ml separating funnel and basify the mixture by cautiously adding 50 per cent aqueous sodium hydroxide. Extract out the liberated amine with three 40 ml portions of ether, dry the extract over anhydrous sodium sulphate, filter and concentrate to about 25 ml using a rotary evaporator.

Methyl Salicylate: Carboxylic Acids and Esters - 2741

2 days ago· The organic layer formed was dried over sodium sulfate, decanted into a pre-weighed 100 ml round-bottom flask, and eventually evaporated using a rotary evaporator. Since the product formed is oil, caution was necessary to prevent the evaporation of the solvent together with the oil. The product formed was weighed and the percent yield determined.

Natural Product Chemistry: Isolation of Caffeine from Tea

rotary evaporator (this is like doing a distillation). Recrystallize the crude caffeine from hexane and acetone. This step Drain the ethyl acetate layer into a clean, dry Erlenmeyer flask and add about 2-3 g of anhydrous sodium sulfate. Swirl occasionally until the sodium sulfate no longer clumps; this should take about 10 minutes.

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